Bruno, Thomas J., Svoronos, P.D.N. 　著

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GAS CHROMATOGRAPHY Carrier Gas Properties New! Carrier Gas Viscosity GasChromatographic Support Materials for Packed Columns Mesh Sizes and ParticleDiameters Packed Column Support Modifiers Properties of ChromatographicColumn Materials Properties of Some Liquid Phases for Packed ColumnsStationary Phases for Packed Column Gas Chromatography Adsorbents forGas-Solid Chromatography Porous Polymer Phases Silicone Liquid PhasesMesogenic Stationary Phases Trapping Sorbents New! Sorbents for theSeparation of Volatile Inorganic Species New! Activated Carbon as a TrappingSorbent for Trace Metals New! Reagent Impregnated Resins as Trapping Sorbentsfor Trace Minerals New! Reagent Impregnated Foams as Trapping Sorbents forInorganic Species New! Chelating Agents for the Analysis of Inorganics by GasChromatography New! Bonded Phase Modified Silica Substrates for Solid PhaseExtraction New! Solid Phase Microextraction Sorbents New! ExtractionCapability of Solid Phase Microextraction Sorbents New! Salting Out Reagentsfor Headspace Analysis New! Partition Coefficients of Common Fluids inAir-Water Systems New! Vapor Pressure and Density of Saturated Water VaporDerivatizing Reagents for Gas Chromatography New! Detectors for GasChromatography New! Recommended Operating Ranges for Hot Wire ThermalConductivity Detectors New! Chemical Compatibility of Thermal ConductivityDetector Wires New! Data for the Operation of Gas Density Detectors New!Phase Ratio for Capillary Columns. New! Martin-James Compressibility Factorand Giddings Plate Height Correction Factor Cryogens for SubambientTemperature Gas Chromatography HIGH PERFORMANCE LIQUID CHROMATOGRAPHY Modesof Liquid Chromatography Solvents for Liquid Chromatography New! Instabilityof HPLC Solvents New! Ultraviolet Absorbance of Reverse Phase Mobile PhasesNew! Ultraviolet Absorbance of Normal Phase Mobile Phases New! Some UsefulIon Pairing Agents New! Materials Compatible with and Resistant to 72 PercentPerchloric Acid More Common HPLC Column Packings Eluotropic Values ofSolvents on Octadecylsilane Mesh Size Relationships New! Efficiency of HPLCColumns New! Column Failure Parameters New! Specialized Stationary Phases forLiquid Chromatography Chiral Stationary Phases for Liquid Chromatography New!Detectors for Liquid Chromatography Ultraviolet Detection of ChromophoricGroups Derivatizing Reagents for HPLC THIN LAYER CHROMATOGRAPHY Strength ofCommon TLC Solvents Modification of the Activity of Alumina by Addition ofWater Stationary and Mobile Phases New! Typical Stationary and Mobile PhaseSystems Used in the Separation of Various Inorganic Ions Spray Reagents inThin Layer Chromatography Protocol for Reagent Preparation SUPERCRITICALFLUID EXTRACTION AND CHROMATOGRAPHY Some Useful Fluids for SupercriticalFluid Extraction and Chromatography P-r-T Table for Carbon Dioxide New!Solubility parameters of the Most Common Fluids for Supercritical FluidExtraction and Chromatography New! Instability of Modifiers used withSupercritical Fluids NEW CHAPTER! ELECTROPHORESIS Separation Ranges ofPolyacrylamide Gels Preparation of Polyacrylamide Gels Buffer MixturesCommonly Used for Polyacrylamide Gel Electrophoresis Proteins for InternalStandardization of Polyacrylamide Gel Electrophoresis Chromogenic Stains forGels Fluorescent Stains for Gels NEW CHAPTER! ELECTROANALYTICAL METHODSDetection Limits for Various Electrochemical Techniques Values of (2.3026RT/F) at Different Temperatures Potential of Zero Charge for VariousElectrode Materials in Aqueous Solutions at Room Temperature Variation ofReference Electrode Potentials with Temperature pH Values of StandardSolutions used in the Calibration of Gas Electrodes Temperature vs. pHCorrelation of Standard Solutions Used for the Calibration of ElectrodesSolid Membrane Electrodes Liquid Membrane Electrodes Standard ReductionElectrode Potentials for Inorganic Systems in Aqueous Solutions at 25oCStandard Reduction Electrode Potentials for Inorganic Systems in Non-AqueousSolutions at 25oC Standard Redox Potentials for Some BiologicalHalf-Reactions Standard E.M.F. Values for the Cell H2 / HCl / AgCl, Ag inVarious Solvents at Different Temperatures Temperature Dependence of theStandard Potential of the Silver Chloride Electrode Standard ElectrodePotentials of Electrodes of the First Kind Standard Electrode Potentials ofElectrodes of the Second Kind Polarographic Half-Wave Potentials (EA ) ofInorganic Cations Polarographic EA Ranges (in V vs. SCE) for the Reductionof Benzene Derivatives Vapor Pressure of Mercury Organic Functional GroupAnalysis of Non-Polarographic Active Groups Coulometric TitrationsULTRAVIOLET SPECTROPHOTOMETRY Solvents for Ultraviolet SpectrophotometryUltraviolet Spectra of Common Liquids Transmittance-Absorbance ConversionCorrelation Table of Ultraviolet Active Functionalities Woodward's Rules forBathochromic Shifts INFRARED SPECTROPHOTOMETRY Infrared Optics MaterialsNew! Internal Reflectance Element Characteristics New! Water Solubility ofInfrared Optics Materials Wavelength-Wavenumber Conversion Table UsefulSolvents for Infrared Spectrophotometry Polystyrene Wavenumber CalibrationInfrared Absorption Correlation Charts New! Aromatic Substitution Bands New!Carbonyl Infrared Absorptions Infrared Absorptions of Major Chemical FamiliesCommon Spurious Infrared Absorption Bands NUCLEAR MAGNETIC RESONANCESPECTROSCOPY Properties of Important NMR Nuclei Gyromagnetic Ratio of SomeImportant Nuclei New! Classification of Important Quadrupolar NucleiAccording to Natural Abundance and Magnetic Strength Chemical Shift Ranges ofSome Nuclei New! Reference Standards for Selected Nuclei New! 1H and 13CChemical Shifts of Useful Solvents for NMR Measurements New! 1H NMRAbsorption of Major Chemical Families Some Useful 1H Coupling ConstantsAdditivity Rules in 13C-NMR Correlation Tables 13C-NMR Absorption of MajorFunctional Groups 13C-NMR Chemical Shifts of Organic Families 15N ChemicalShifts for Common Standards 15N Chemical Shifts of Major Chemical Families15N Spin-Spin Coupling 19F Chemical Shift Ranges 19F Chemical Shifts of SomeFluorine-Containing Compounds 19F Coupling Constants New! Residual PeaksObserved in the 1H NMR Spectra of Common Deuterated Organic Solvents MASSSPECTROSCOPY Natural Abundance of Important Isotopes Rules for Determinationof Molecular Formula New! Neutral Moieties Ejected from Substituted BenzeneRing Compounds New! Order of Fragmentation Initiated by the Presence of aSubstituent on a Benzene Ring Chlorine-Bromine Combination IsotopeIntensities Reference Compounds Under Electron Impact Conditions in MassSpectroscopy Major Reference Masses in the Spectrum ofHeptacosafluorotributylamine Common Fragmentation Patterns of Families ofOrganic Compounds Common Fragments Lost Important Peaks in the Mass Spectraof Common Solvents New! Reagent Gases for Chemical Ionization MassSpectrometry Proton Affinity of Reactant Gases in Chemical Ionization MassSpectrometry Proton Affinities of Some Simple Molecules Proton Affinities ofSome Anions New! Detection of Leaks in Mass Spectrometers New! MassResolution Required to Resolve Common Spectral Interferences Encountered inInductively Coupled Plasma Mass Spectrometry (ICP-MS) ATOMIC ABSORPTIONSPECTROMETRY Introduction for Atomic Spectrometric Tables StandardSolutions-Selected Compounds and Procedures Limits of Detection for CommonAnalytical Transitions in AES and AAS Detection Limits by Hydride Generationand Cold Vapor AAS Spectral Overlaps Relative Intensities of ElementalTransitions from Hollow Cathode Lamps Neon HCl Spectrum Neon Lines Which Mustbe Resolved for Accurate AAS Measurements Argon HCl Spectrum Argon LinesWhich Must be Resolved for Accurate AAS Measurements Close Lines forBackground Correction Beta Values for the Air-Acetylene and NitrousOxide-Acetylene Flames Lower Energy Level Populations (in percent) as aFunction of Temperature Critical Optimization Parameters for AES/AAS MethodsFlame Temperatures and References on Temperature Measurements FundamentalData for the Common Transitions New! Activated Carbon as a Trapping Sorbentfor Trace Metals. New! Reagent Impregnated Resins as Trapping Sorbents forInorganic Species New! Reagent Impregnated Foams as Trapping Sorbents forInorganic Species QUALITATIVE TESTS Organic Group Qualitative TestsInorganic Group Qualitative Tests Organic Precipitation for Inorganic IonsNEW CHAPTER! SOLUTION PROPERTIES Physical Properties of Water. RefractiveIndex of Water Approximate pK Values of Compounds Useful in Buffer SystemsPreparation of Buffers Dielectric Constants of Inorganic Solvents DielectricConstants of Methanol-Water Mixtures from 5 - 55oC Common Drying Agents forOrganic Liquids Common Recrystallization Solvents NEW CHAPTER! TABLES FORLABORATORY SAFETY Major Chemical Incompatibilities Materials Compatible withand Resistant to 72 Percent Perchloric Acid Properties of Hazardous SolidsCompounds that are Reactive with Water Pyrophoric Compounds - Compounds thatare Reactive with Air Vapor Pressure of Mercury Flammability Hazards ofCommon Liquids Chemical Carcinogens Organic Peroxides Characteristics ofChemical Resistant Materials Selection of Protective Laboratory GarmentsSelection of Laboratory Gloves Selection of Respirator Cartridges and FiltersEffects of Electrical Current on the Human Body Electrical Requirements ofCommon Laboratory Devices MISCELLANEOUS TABLES Unit Conversions New! Massand Volume Based Concentration Units Prefixes for SI Units Updated!Recommended Values of Physical Constants Standards for Laboratory WeightsNew! Thermocouple Reference Voltages New! Standard CGA Fittings forCompressed Gas Cylinders New! Gas Cylinder Stamped Markings New! ElectricalOutlet and Plug Formats